Hydrazine → 8-Piperidinyloctylamine

HRID 1463824Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1463824
[NH2:1]N.[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16]C2C=CC=C3C(NC(=O)C=23)=O)[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1>CO>[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][NH2:1])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]1

Komponenten

4

Edukt 2

HCID 9321HydrazineHCID 540305088-Piperidinyloctylphthalimide

Produkt 1

HCID 110092698-Piperidinyloctylamine

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 8-piperidinyloctylphthalimide (274 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

Aufarbeitung

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

Quellen und Nachweise

ORD-Eintrag
ord-7b07b0fd85c84a33a3b59b3d7d5fd1eb
Quelldatensatz
uspto-grants-1994_04
Patentnummer
US05302593

Notizen zur Reaktion

Wird geladen…