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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1464711Erstellt: 26. Oktober 2026

Aluminum(III) Chloride → 1-Chloro-2,4-dimethylbenzene

https://huagongshe.com/reaction/1464711

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAluminum(III) ChlorideHCID 6451240—
Edukt2,4-Dimethylphenyl chloroformateHCID 15917593—
Produkt1-Chloro-2,4-dimethylbenzeneHCID 52315320%

Reaktionsbedingungen

Temperatur200 °C

Reaktionsschritte

0.5 g of anhydrous aluminium chloride was added to 15 g of 2,4-dimethylphenyl chloroformate and the mixture was heated at 200° C. for 3 hours at normal pressure. The reaction mixture was cooled and worked up as described in Example 1. 2,4-Dimethylchlorobenzene was obtained in a yield of 20%, which is considerable despite the unfavourable substitution pattern.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05306849
Quelldatensatzuspto-grants-1994_04
ORD IDord-12fece4313ed4ea2ba676f655f6f6b57
Quellennotizuspto-grants-1994_04