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HRID 1464711Erstellt: 26. Oktober 2026
Aluminum(III) Chloride → 1-Chloro-2,4-dimethylbenzene
https://huagongshe.com/reaction/1464711
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
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| Edukt | Aluminum(III) Chloride | HCID 6451240 | — |
| Edukt | 2,4-Dimethylphenyl chloroformate | HCID 15917593 | — |
| Produkt | 1-Chloro-2,4-dimethylbenzene | HCID 523153 | 20% |
Reaktionsschritte
0.5 g of anhydrous aluminium chloride was added to 15 g of 2,4-dimethylphenyl chloroformate and the mixture was heated at 200° C. for 3 hours at normal pressure. The reaction mixture was cooled and worked up as described in Example 1. 2,4-Dimethylchlorobenzene was obtained in a yield of 20%, which is considerable despite the unfavourable substitution pattern.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US05306849 |
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| Quelldatensatz | uspto-grants-1994_04 |
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| ORD ID | ord-12fece4313ed4ea2ba676f655f6f6b57 |
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| Quellennotiz | uspto-grants-1994_04 |
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