Reaktionsgleichung
ClC(O[C:5]1[C:10]([CH3:11])=[CH:9][CH:8]=[CH:7][C:6]=1[CH3:12])=O.[FH:13]>>[CH3:12][C:6]1[CH:7]=[CH:8][CH:9]=[C:10]([CH3:11])[C:5]=1[F:13]Komponenten
3
Versuchsvorschrift
1000 ml of anhydrous hydrogen fluoride were placed at 0° C. in a stainless steel laboratory autoclave and 500 g of 2,6-dimethylphenyl chloroformate were added dropwise. The reaction was carried out and the reaction mixture worked up as described in Example 9. 2,6-Dimethylfluorobenzene was obtained in a yield of 51%.
Aufarbeitung
- additionwere added dropwise
Quellen und Nachweise
- ORD-Eintrag
- ord-815b8636b4344f7db94ab8dea359cbc5
- Quelldatensatz
- uspto-grants-1994_04
- Patentnummer
- US05306849
Verknüpfte Notizen
Wird geladen…