Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Antimony pentafluoride | HCID 24557 | — |
| Edukt | 2,6-Dimethylphenylfluoroformate | HCID 10844827 | — |
| Produkt | 2-Fluoro-m-xylene | HCID 123065 | 40% |
Reaktionsschritte
3.9 g of antimony pentafluoride were added to 100 g of 2,6-dimethylphenyl fluoroformate and the mixture was heated at 200° C. for 5 hours at normal pressure. The reaction mixture was then cooled and worked up as described in Example 1. 2,6-Dimethylfluorobenzene was obtained in a yield of 40%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US05306849 |
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| Quelldatensatz | uspto-grants-1994_04 |
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| ORD ID | ord-baa92f8612094a66b8c28eae6b5d3051 |
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| Quellennotiz | uspto-grants-1994_04 |
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