Ethanol → 3-(2-Oxo-propylsulfanyl)-benzoic acid ethyl ester

HRID 1466821Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1466821
[O:1]=[C:2]([CH3:14])[CH2:3][S:4][C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][CH:13]=1)[C:8]([OH:10])=[O:9].OS(O)(=O)=O.[CH2:20](O)[CH3:21]>>[CH2:20]([O:9][C:8](=[O:10])[C:7]1[CH:11]=[CH:12][CH:13]=[C:5]([S:4][CH2:3][C:2](=[O:1])[CH3:14])[CH:6]=1)[CH3:21]

Komponenten

4

Edukt 3

HCID 702EthanolHCID 1118Sulfuric AcidHCID 667650833-(2-Oxo-propylsulfanyl)-benzoic acid

Produkt 1

HCID 667651013-(2-Oxo-propylsulfanyl)-benzoic acid ethyl ester

Versuchsvorschrift

3-(2-Oxo-propylsulfanyl)-benzoic acid from the previous reaction was dissolved in ethanol and a catalytic amount of conc. H2SO4 was added. The reaction was monitored by analytical TLC and when it was complete the reaction was concentrated to dryness and the resulting residue was purified via silica gel chromatography to give the title compound.

Aufarbeitung

  1. concentrationwas concentrated to dryness
  2. customthe resulting residue was purified via silica gel chromatography

Quellen und Nachweise

ORD-Eintrag
ord-9d8e3d678b22485cadca128bc1209fc9
Quelldatensatz
uspto-grants-2015_04
Patentnummer
US09000025B2

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