Benzoyl isocyanate → HCID 66745827, Verbindung
Reaktionsgleichung
[NH2:1][C:2]1[C:3]([C:19]#[N:20])=[C:4]([CH:16]=[CH:17][CH:18]=1)[O:5][CH2:6][C:7]([CH3:15])([CH3:14])[C:8]([NH:10][CH2:11][CH2:12][CH3:13])=[O:9].[C:21]([N:29]=[C:30]=[O:31])(=[O:28])[C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1>>[C:19]([C:3]1[C:4]([O:5][CH2:6][C:7]([CH3:15])([CH3:14])[C:8](=[O:9])[NH:10][CH2:11][CH2:12][CH3:13])=[CH:16][CH:17]=[CH:18][C:2]=1[NH:1][C:30]([NH:29][C:21](=[O:28])[C:22]1[CH:23]=[CH:24][CH:25]=[CH:26][CH:27]=1)=[O:31])#[N:20]Komponenten
3
Versuchsvorschrift
Prepared as in Example 24a from 3-(3-amino-2-cyanophenoxy)-2,2-dimethyl-N-propylpropanamide (Example 197b, Method A) and benzoyl isocyanate in 85% yield as a white solid. MS 423 (MH+).
Quellen und Nachweise
- ORD-Eintrag
- ord-e30823d8a29140e8b331c85537233a02
- Quelldatensatz
- uspto-grants-2015_04