Potassium Carbonate → Ethyl 4-(benzyloxy)-3-hydroxybenzoate

HRID 1475729Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1475729
[CH2:1]([O:3][C:4](=[O:23])[C:5]1[CH:10]=[CH:9][C:8]([O:11][CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[C:7]([O:19]C(=O)C)[CH:6]=1)[CH3:2].C(=O)([O-])[O-].[K+].[K+]>CO>[CH2:1]([O:3][C:4](=[O:23])[C:5]1[CH:10]=[CH:9][C:8]([O:11][CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[C:7]([OH:19])[CH:6]=1)[CH3:2]

Komponenten

4

Edukt 2

HCID 11430Potassium CarbonateHCID 67170201HCID 67170201, Verbindung

Produkt 1

HCID 11311797Ethyl 4-(benzyloxy)-3-hydroxybenzoate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

The compound of step 2 (10 g, 31.8 mmol) was dissolved in methanol, potassium carbonate (88 mg, 0.636 mmol) was added and the mixture was stirred for 2 h under reflux. The solution was evaporated to dryness and the residue used without further purification.

Aufarbeitung

  1. temperatureunder reflux
  2. customThe solution was evaporated to dryness
  3. customthe residue used without further purification

Quellen und Nachweise

ORD-Eintrag
ord-d90752650c4f472285caa383b64c714a
Quelldatensatz
uspto-grants-2015_04
Patentnummer
US09018383B2

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