HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sulfuric Acid → 2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide sulfate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sulfuric Acid | HCID 1118 | — |
| Edukt | 2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide | HCID 71811587 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | 2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide sulfate | HCID 118387004 | 72% |
Reaktionsschritte
2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide dissolved in EA, stirred at room temperature, while dropped H2SO4 into mixture till occurred to white solid. The reaction mixture was filtered to get White solid; 72% yield;
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09402819B2 |
| Quelldatensatz | uspto-grants-2016_08 |
| ORD ID | ord-46c5fcb07c94481a8e8f0d3a8d9e85a9 |
| Quellennotiz | uspto-grants-2016_08 |