Ammonia → 3-Amino-1,2,4-triazine mesylate

HRID 1484496Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1484496
C(OC1C=C(C=[CH:17][CH:18]=1)C(OC)=O)C1C=CC=CC=1.[S:19]([OH:23])(=[O:22])(=[O:21])[CH3:20].S(O)(=O)(=O)C.[NH2:29][NH:30][C:31]([NH2:33])=[NH:32].N>>[S:19]([OH:23])(=[O:22])(=[O:21])[CH3:20].[NH2:33][C:31]1[N:30]=[N:29][CH:17]=[CH:18][N:32]=1

Komponenten

4

Edukt 3

HCID 222AmmoniaHCID 13368031Methyl 3-(benzyloxy)benzoateHCID 178505340HCID 178505340, Verbindung

Produkt 1

HCID 866497313-Amino-1,2,4-triazine mesylate

Versuchsvorschrift

Prepared by reacting acenaphthenequinone (3) with aminoguanidine bismesylate for 24 hrs using the above procedure except that the basification step with ammonia was omitted. The title compound was obtained as bright yellow prisms in 83.2%, mpt=264-266° (froth)

Aufarbeitung

  1. customPrepared
  2. customfor 24 hrs

Quellen und Nachweise

ORD-Eintrag
ord-a8de5f0905094df09005f1c293579976
Quelldatensatz
uspto-grants-2016_08
Patentnummer
US09422253B2

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