Thionyl Chloride → 3-Iodo-2-methoxy-benzoyl chloride
Reaktionsgleichung
[I:1][C:2]1[C:3]([O:11][CH3:12])=[C:4]([CH:8]=[CH:9][CH:10]=1)[C:5](O)=[O:6].S(Cl)([Cl:15])=O>>[I:1][C:2]1[C:3]([O:11][CH3:12])=[C:4]([CH:8]=[CH:9][CH:10]=1)[C:5]([Cl:15])=[O:6]Komponenten
3
Reaktionsbedingungen
- Temperatur
- 82 °C
Versuchsvorschrift
To 3-iodo-2-methoxy-benzoic acid (8.29 g, 29.8 mmol) was added thionyl chloride (15 mL). The resulting solution was stirred for 2 minutes then heated to 82° C. and stirred at this temperature for 30 minutes. The solution was then concentrated under reduced pressure to give the title compound. This material was used without further purification.
Aufarbeitung
- stirringstirred at this temperature for 30 minutes
- concentrationThe solution was then concentrated under reduced pressure
Quellen und Nachweise
- ORD-Eintrag
- ord-daa4fe77befb488383dc64d10e0c2f9c
- Quelldatensatz
- uspto-grants-2016_08
- Patentnummer
- US09422314B2
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