HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
ethyl 2-methyl-1H-indole-3-carboxylate → Ethyl 2-methyl-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-YL)-1H-indole-3-carboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | ethyl 2-methyl-1H-indole-3-carboxylate | HCID 4072358 | — |
| Reagenz | Bis(pinacolato)diborane | HCID 2733548 | — |
| Reagenz | 4,4'-Di-tert-butyl-2,2'-bipyridyl | HCID 4249187 | — |
| Katalysator | Bis(1,5-cyclooctadiene)dimethoxydiiridium | HCID 76001521 | — |
| Lösungsmittel | Hexane | HCID 8058 | — |
| Produkt | Ethyl 2-methyl-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-YL)-1H-indole-3-carboxylate | HCID 24960599 | 64% |
Reaktionsbedingungen
| Temperatur | 60 °C |
|---|
Herkunft & Nachweise
| DOI | 10.1021/ja0631652 |
|---|---|
| Quelldatensatz | Borylation dataset from Roche |
| ORD ID | ord-76f888b89be1471b8f20bbaec2a532c5 |
| Quellennotiz | Borylation dataset from Roche |