HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,5-Dichloro-3-nitrobenzoic acid → 2,5-Dichloro-3-nitrobenzoyl chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,5-Dichloro-3-nitrobenzoic acid | HCID 6951 | — |
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Produkt | 2,5-Dichloro-3-nitrobenzoyl chloride | HCID 10106386 | 87,5% |
Reaktionsschritte
A mixture of 5.0 parts of 2,5-dichloro-3-nitrobenzoic acid and 16.2 parts of thionyl chloride was refluxed for 24 hours under argon. The reaction mixture was evaporated, yielding 4.74 parts (87.5%) of 2,5-dichloro-3-nitrobenzoyl chloride (interm. 66).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05371079 |
| Quelldatensatz | uspto-grants-1994_12 |
| ORD ID | ord-93a1812400df4f5a9a075dd26cbecb43 |
| Quellennotiz | uspto-grants-1994_12 |