Hydrochloric Acid → 1H,2H,3H-pyrrolo(3,4-c)pyridine dihydrochloride

HRID 1491655Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1491655
[CH2:1]1[C:9]2[CH:8]=[CH:7][N:6]=[CH:5][C:4]=2[CH2:3][N:2]1C(OCC)=O.[ClH:15]>>[ClH:15].[ClH:15].[CH2:1]1[C:9]2[CH:8]=[CH:7][N:6]=[CH:5][C:4]=2[CH2:3][NH:2]1

Komponenten

3

Edukt 2

HCID 313Hydrochloric AcidHCID 18953633ethyl 1H-pyrrolo[3,4-c]pyridine-2(3H)-carboxylate

Produkt 1

HCID 189536441H,2H,3H-pyrrolo(3,4-c)pyridine dihydrochloride

Versuchsvorschrift

10.4 g (51 mmol) of ethyl 2,3-dihydro-1H-pyrrolo-[3,4-c]pyridine-2-carboxylate are refluxed for 15 hours together with 100 ml of concentrated hydrochloric acid. The batch is evaporated, and the crystalline residue is stirred with acetone. The product is filtered off with suction and dried in the air.

Aufarbeitung

  1. customThe batch is evaporated
  2. filtrationThe product is filtered off with suction
  3. customdried in the air

Quellen und Nachweise

ORD-Eintrag
ord-e690b9584d3b46ad8e37691ab0bf9ae7
Quelldatensatz
uspto-grants-1994_12
Patentnummer
US05371090

Notizen zur Reaktion

Wird geladen…