Propionitrile → HCID 178458050, Verbindung

Reaktionsgleichung

[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[N:8]1[CH2:13][CH2:12][O:11][CH2:10][CH2:9]1.[C:14](#[N:17])[CH2:15][CH3:16].[Cl-].[Al+3].[Cl-].[Cl-]>>[O:11]1[CH2:12][CH2:13][N:8]([C:3]2[CH:4]=[CH:5][CH:6]=[CH:7][C:2]=2[NH:1][C:14](=[NH:17])[CH2:15][CH3:16])[CH2:9][CH2:10]1

Komponenten

Edukt 3

HCID 7854Propionitrile

HCID 7357562-Morpholinoaniline

HCID 6451240Aluminum(III) Chloride

Produkt 1

HCID 178458050HCID 178458050, Verbindung

Versuchsvorschrift

A mixture of 4-(2-aminophenyl)morpholine (5.34 g), propionitrile (4.7 g) and anhydrous aluminium chloride (12 g) was heated at 160°-170° C. for six hours to yield N-(2-morpholinophenyl)propionamidine (m.p. 114° C.) which was recrystallised from hexane.