Methyl iodide → HCID 178503978, Verbindung

HRID 1492211Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1492211
[O:1]1[CH2:6][CH2:5][N:4]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=2[NH:13][C:14]([NH2:16])=[S:15])[CH2:3][CH2:2]1.[CH3:17][I:18]>CO>[IH:18].[CH3:17][S:15][C:14](=[NH:16])[NH:13][C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=1[N:4]1[CH2:5][CH2:6][O:1][CH2:2][CH2:3]1

Komponenten

4

Edukt 2

HCID 6328Methyl iodideHCID 27411931-(2-Morpholinophenyl)thiourea

Produkt 1

HCID 178503978HCID 178503978, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

A solution of 1-(2-morpholinophenyl)thiourea (7.2 g) in dry methanol (30 ml) was heated at reflux with methyliodide (4.2 g) for 2 hours. The solvent was removed under reduced pressure and dry ether (15 ml) was added and on scratching gave 2-methyl-1-(2-morpholinophenyl)-2-thiopseudourea hydroiodide (m.p. 151°-152° C.).

Aufarbeitung

  1. customThe solvent was removed under reduced pressure and dry ether (15 ml)
  2. additionwas added

Quellen und Nachweise

ORD-Eintrag
ord-cad3fee50b7346f5b53ce7976e22d40d
Quelldatensatz
uspto-grants-1994_12
Patentnummer
US05373008

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