Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Acetone, oxime | HCID 67180 | — |
| Edukt | 4-{3-[4-(1-Chloroethyl)phenylthio]-5-fluorophenyl}-4-methoxytetrahydropyran | HCID 19379931 | — |
| Produkt | HCID 9909885 | HCID 9909885 | 58% |
Reaktionsschritte
Using an analogous procedure to that described in Example 1 except that the reactants were heated to 60° C. for 2 hours, acetone oxime was reacted with 4-{3-[4-(1-chloroethyl)phenylthio]-5-fluorophenyl}-4-methoxytetrahydropyran to give acetone O-{4-[5-fluoro-3-(4-methoxytetrahydropyran-4-yl)phenylthio)-α-methylbenzyl}oxime as an oil in 58% yield.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US05376680 |
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| Quelldatensatz | uspto-grants-1994_12 |
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| ORD ID | ord-eb32913a49604aa78cf550693e028e28 |
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| Quellennotiz | uspto-grants-1994_12 |
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