Chlorosulfamic acid → 2-(4-Chlorophenoxy)-2-methylpropanol sulfamate
Reaktionsgleichung
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[Cl:6][C:7]1[CH:18]=[CH:17][C:10]([O:11][C:12]([CH3:16])([CH3:15])[CH2:13][OH:14])=[CH:9][CH:8]=1>>[Cl:6][C:7]1[CH:18]=[CH:17][C:10]([O:11][C:12]([CH3:15])([CH3:16])[CH2:13][O:14][S:1](=[O:4])(=[O:3])[NH2:2])=[CH:9][CH:8]=1Komponenten
3
Versuchsvorschrift
The title compound was prepared by procedures of Example 16 from sulfamoyl chloride and 2-(4-chlorophenoxy)-2-methylpropanol to give a white solid, mp 76°-79° C., in 58% yield.
Aufarbeitung
- customto give a white solid, mp 76°-79° C.
Quellen und Nachweise
- ORD-Eintrag
- ord-9ae764c394e54e089e709db3f3b6be05
- Quelldatensatz
- uspto-grants-1991_06
- Patentnummer
- US05025031
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