HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Toluene → 2-Chlorophenyl sulfamate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Toluene | HCID 1140 | — |
| Edukt | 2-Chlorophenol | HCID 7245 | — |
| Edukt | Chlorosulfonyl isocyanate | HCID 70918 | — |
| Lösungsmittel | Benzene--cyclohexane (1/1) | HCID 18624872 | — |
| Produkt | 2-Chlorophenyl sulfamate | HCID 21694498 | 59% |
Reaktionsschritte
This compound was prepared by the procedure used in Example 56. A mixture of 12.8 g (0.1 mole) of 2-chlorophenol, 14.8 g (0.105 mole) of chlorosulfonyl isocyanate and 75 ml of toluene gave 12.2 g (59%) of the title compound as a white solid, mp 62.5°-63.5° C. (cyclohexane-benzene).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05025031 |
| Quelldatensatz | uspto-grants-1991_06 |
| ORD ID | ord-bc803db57946496e9e3cf290c4128f56 |
| Quellennotiz | uspto-grants-1991_06 |