Thionyl Chloride → HCID 53915754, Verbindung

HRID 1494600Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1494600
[CH:1]([C:3]1([C:12]([OH:14])=O)[CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4]1)=[CH2:2].S(Cl)([Cl:17])=O>>[CH:1]([C:3]1([C:12]([Cl:17])=[O:14])[CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4]1)=[CH2:2]

Komponenten

3

Edukt 2

HCID 24386Thionyl ChlorideHCID 19828700HCID 19828700, Verbindung

Produkt 1

HCID 53915754HCID 53915754, Verbindung

Versuchsvorschrift

A mixture 2,3-dihydro-2-vinyl-1H-indene-2-carboxylic acid (5.09 g) and thionyl chloride (25 ml) was refluxed for 10 hours. Excess thionyl chloride was distilled off under reduced pressure. The crude product was used as such for the following reaction.

Aufarbeitung

  1. distillationExcess thionyl chloride was distilled off under reduced pressure
  2. customsuch for the following reaction

Quellen und Nachweise

ORD-Eintrag
ord-89f5ee2aa9fd40c395f9ef973cc3e60a
Quelldatensatz
uspto-grants-1991_06
Patentnummer
US05026868

Notizen zur Reaktion

Wird geladen…