Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1496945Erstellt: 24. Oktober 2026

Potassium Carbonate → 1-(4-(3-Ethoxy-4-nitrophenyl)piperazin-1-yl)ethanone

https://huagongshe.com/de/reaction/1496945

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPotassium CarbonateHCID 11430—
Edukt1-AcetylpiperazineHCID 83795—
Edukt2-Ethoxy-4-fluoronitrobenzeneHCID 12918153—
LösungsmittelDimethylformamideHCID 6228—
Produkt1-(4-(3-Ethoxy-4-nitrophenyl)piperazin-1-yl)ethanoneHCID 118105754—

Reaktionsschritte

The compound obtained in Step 1 above (300 mg), N-acetylpiperazine (300 mg), and potassium carbonate (500 mg) were dissolved in dimethylformamide (3 mL) and reacted at 80° C. overnight. The dimethylformamide of the reaction mixture was removed under reduced pressure, and added with water to form a solid. The solid was filtered to obtain a target compound as a yellow solid.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS09199944B2
Quelldatensatzuspto-grants-2015_12
ORD IDord-2c8e1a83285440b6b1edfc06111e3ca8
Quellennotizuspto-grants-2015_12