Reaktionsgleichung
[CH2:1]([O:8][C:9]1[CH:14]=[CH:13][N:12]([C:15]2[CH:20]=[CH:19][C:18]([OH:21])=[CH:17][CH:16]=2)[C:11](=[O:22])[CH:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[F:23]C(OC1C=CN(C2C=CC(O)=CC=2)C(=O)C=1)C1C=CC=CC=1.[N:46]([CH2:49][CH2:50]O)=[N+:47]=[N-:48]>>[F:23][C:5]1[CH:6]=[CH:7][C:2]([CH2:1][O:8][C:9]2[CH:14]=[CH:13][N:12]([C:15]3[CH:16]=[CH:17][C:18]([O:21][CH2:50][CH2:49][N:46]=[N+:47]=[N-:48])=[CH:19][CH:20]=3)[C:11](=[O:22])[CH:10]=2)=[CH:3][CH:4]=1Komponenten
4
Versuchsvorschrift
Step (3) of Example 12 was repeated except that 4-benzyloxy-1-(4-hydroxyphenyl)-1H-pyridin-2-one and 2-(1-pyrrolidine)ethanol were replaced with 4-(4-(fluorobenzyloxy)-1-(4hydroxyphenyl)-1H-pyridin-2-one (Step (2) of Example 28) and 2-azidoethanol, respectively, to provide the title compound.
Quellen und Nachweise
- ORD-Eintrag
- ord-062ca5ed8b7c4f5997ef176e6eeee92b
- Quelldatensatz
- uspto-grants-2010_06
- Patentnummer
- US07732456B2
Verknüpfte Notizen
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