HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Water → Salvinorin B
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Water | HCID 962 | — |
| Edukt | Sodium Carbonate | HCID 10340 | — |
| Edukt | Salvinorin A | HCID 128563 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | Salvinorin B | HCID 11440685 | 42,3% |
Reaktionsschritte
To a solution of Salvinorin A (500 mg, 1.15 mM) in methanol (10 ml) was added solid sodium carbonate (490 mg, 4.6 mM) and the mixture stirred at room temperature overnight. Water (20 ml) was added to mixture and the mixture stirred for 30 mins. The solution was filtered and the filter-cake washed with ice-cold water (20 ml) and ice-cold methanol (20 ml) and dried in a dessicator to give Salvinorin B (191 mg, 42%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09222949B2 |
| Quelldatensatz | uspto-grants-2015_12 |
| ORD ID | ord-fde16edeb1b248fdb5fe3b8ab8ff05a5 |
| Quellennotiz | uspto-grants-2015_12 |