Methanol → Nitrophenoxyacetone
Reaktionsgleichung
[N+:1]([C:4]1C=CC=[CH:11][C:5]=1[O:6]CC(=O)C)([O-:3])=[O:2].[C:15]1(C)[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1.C[OH:23]>>[N+:1]([CH:4]([O:23][C:15]1[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=1)[C:5](=[O:6])[CH3:11])([O-:3])=[O:2]Komponenten
4
Versuchsvorschrift
2624 g of o-nitrophenoxyacetone crystals (˜98%) from the 1st stage, step d), were dissolved at room temperature in a mixture of 11 307 g of methanol and 1290 g of toluene at 40° C., in order to obtain an about 17.6% solution of nitrophenoxyacetone.
Quellen und Nachweise
- ORD-Eintrag
- ord-4897176cdc784cb6a0b5a49820a27440
- Quelldatensatz
- uspto-grants-2012_07
- Patentnummer
- US08222408B2
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