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HRID 1518174Erstellt: 27. Oktober 2026

Benzyloxy-acetic acid 5-chloro-2-(2,4-dichloro-phenoxy)-phenyl ester → Hydroxy-acetic acid 5-chloro-2-(2,4-dichloro-phenoxy)-phenyl ester

https://huagongshe.com/reaction/1518174

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzyloxy-acetic acid 5-chloro-2-(2,4-dichloro-phenoxy)-phenyl esterHCID 57667396—
KatalysatorPalladiumHCID 23938—
LösungsmittelMethanolHCID 887—
ProduktHydroxy-acetic acid 5-chloro-2-(2,4-dichloro-phenoxy)-phenyl esterHCID 57667367—

Reaktionsschritte

Benzyloxy-acetic acid 5-chloro-2-(2,4-dichloro-phenoxy)-phenyl ester 4 (5 grams) was dissolved in methanol (50 mL) in a pressure vessel, palladium on carbon (5%, 5 grams) was added and the mixture was stirred under an atmosphere of hydrogen (4 Kg) for 4 hours. The catalyst was removed by filtration and the methanol was distilled off to yield crude 5.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08232422B2
Quelldatensatzuspto-grants-2012_07
ORD IDord-3a5c37b98057400886749780a484c000
Quellennotizuspto-grants-2012_07