HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3,5-Dibromosalicylaldehyde → HCID 178449914, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3,5-Dibromosalicylaldehyde | HCID 7024 | — |
| Edukt | N-tert-butylhydroxylamine | HCID 98586 | — |
| Produkt | HCID 178449914 | HCID 178449914 | — |
Reaktionsschritte
The title compound was prepared according to the procedure described in Example 13 using 3,5-dibromo-2-hydroxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 68.7% yield as a yellow crystalline solid, m.p. 111.3° C. (Rf=0.54 on a silica gel plate using 7:3 hexanes/EtOAc as an eluant).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06197826B1 |
| Quelldatensatz | uspto-grants-2001_03 |
| ORD ID | ord-5175da832f654f48a85633dbe044f612 |
| Quellennotiz | uspto-grants-2001_03 |