HCID 9846158, Verbindung → HCID 9869673, Verbindung

HRID 1532645Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1532645
[ClH:1].C(OCC)(=O)C.[CH2:8]([C:25]1[N:29]([CH2:30][CH2:31][CH2:32][N:33]([CH3:35])[CH3:34])[C:28]2[CH:36]=[CH:37][CH:38]=[CH:39][C:27]=2[N:26]=1)[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]>C(OCC)(=O)C>[ClH:1].[CH2:8]([C:25]1[N:29]([CH2:30][CH2:31][CH2:32][N:33]([CH3:34])[CH3:35])[C:28]2[CH:36]=[CH:37][CH:38]=[CH:39][C:27]=2[N:26]=1)[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]

Komponenten

4

Edukt 2

HCID 9846158HCID 9846158, VerbindungHCID 21866389Hydrogen chloride-ethyl acetate

Produkt 1

HCID 9869673HCID 9869673, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 8857Ethyl AcetateLösungsmittel

Versuchsvorschrift

4N Hydrochloric acid/ethyl acetate solution (0.19 ml) was added to a solution containing 3-(2-heptadecyl-1H-benzimidazol-1-yl)-N,N-dimethyl-1-propanamine (0.33 g) in ethyl acetate (5 ml). After being stirred for 10 minutes at room temperature, the reaction mixture was concentrated. The residue was recrystallized with ethyl acetate, thereby yielding the entitled compound (0.32 g) as white solid.

Aufarbeitung

  1. concentrationthe reaction mixture was concentrated
  2. customThe residue was recrystallized with ethyl acetate

Quellen und Nachweise

ORD-Eintrag
ord-9200d9f4de064ba08d6153b591ed8acc
Quelldatensatz
uspto-grants-2001_03
Patentnummer
US06204264B1

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