HCID 3635836, Verbindung → HCID 22013772, Verbindung

HRID 1532652Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1532652
[O:1]1[CH2:6][CH2:5][N:4]([CH2:7][CH2:8][CH2:9][NH:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=2[N+:17]([O-])=O)[CH2:3][CH2:2]1>C(O)C.[C].[Pd]>[O:1]1[CH2:2][CH2:3][N:4]([CH2:7][CH2:8][CH2:9][NH:10][C:11]2[C:12]([NH2:17])=[CH:13][CH:14]=[CH:15][CH:16]=2)[CH2:5][CH2:6]1

Komponenten

4

Edukt 1

HCID 3635836HCID 3635836, Verbindung

Produkt 1

HCID 22013772HCID 22013772, VerbindungAusbeute 72,3 %

Reagenzien, Katalysatoren, Lösungsmittel 2

HCID 178418390HCID 178418390, VerbindungKatalysatorHCID 702EthanolLösungsmittel

Versuchsvorschrift

10% of palladium-carbon (0.237 g) was added to a solution containing N-(3-morpholinopropyl)-2-nitroaniline (1.040 g) in ethanol (12 ml) and the mixture was stirred for 7 hours under a hydrogen gas atmosphere at room temperature. After the catalyst was removed out by filtration, the filtrate was concentrated, thereby yielding the entitled compound (0.667 g) as blackish brown solid.

Aufarbeitung

  1. customAfter the catalyst was removed out by filtration
  2. concentrationthe filtrate was concentrated

Quellen und Nachweise

ORD-Eintrag
ord-1a6fd057d8774fbebee166422eacf186
Quelldatensatz
uspto-grants-2001_03
Patentnummer
US06204264B1

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