HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-(4-Ethylaminophenyl)-4-phenylmethylpiperazine → 1-(4-Ethylaminophenyl)piperazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-(4-Ethylaminophenyl)-4-phenylmethylpiperazine | HCID 19911465 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 1-(4-Ethylaminophenyl)piperazine | HCID 19911458 | — |
Reaktionsschritte
A solution of 1-(4-ethylaminophenyl)-4-phenylmethylpiperazine in ethanol is catalytically hydrogenated at about 70° C. and 50 p.s.i., in the presence of 10% palladium on carbon. After hydrogen uptake ceases, the catalyst is removed by filtration and the filtrate concentrated to obtain the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05086055 |
| Quelldatensatz | uspto-grants-1992_02 |
| ORD ID | ord-590c27b31dff476298179a48dbf18bb1 |
| Quellennotiz | uspto-grants-1992_02 |