HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl Stearate → Potassium Stearate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl Stearate | HCID 8201 | — |
| Edukt | Potassium Hydroxide | HCID 14797 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | Potassium Stearate | HCID 23673840 | — |
Reaktionsschritte
44.8 grams of methyl stearate (0.75 moles/mole of sucrose to be used in Step B) is saponified by stirring at reflux in 200 ml methanol containing an equivalent amount of KOH (9.4 grams of 90% purity). The reaction is stirred at 60° C. for about an hour with heating until all methyl ester has been converted to soap as indicated by infrared analysis. The soap solution is used, as is, in the next reaction step.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05085884 |
| Quelldatensatz | uspto-grants-1992_02 |
| ORD ID | ord-b5d438440b8143f6947c62fbf9aa287b |
| Quellennotiz | uspto-grants-1992_02 |