N-methyl-2-pyrrolidone → S-octadecyl thiocarbamate

HRID 1535002Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1535002
[CH2:1]([SH:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].C[N:21]1CCC[C:22]1=[O:26]>>[C:22](=[O:26])([S:19][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])[NH2:21]

Komponenten

3

Edukt 2

HCID 13387N-methyl-2-pyrrolidoneHCID 179051-Octadecanethiol

Produkt 1

HCID 18997609S-octadecyl thiocarbamateAusbeute 60 %

Versuchsvorschrift

As described in Example 17, but using 63 g of 1-octadecylmercaptan (0.22 mol) dissolved in 30 ml of N-methylpyrrolidone, S-octadecyl thiocarbamate was obtained in a yield of 60% of theory.

Quellen und Nachweise

ORD-Eintrag
ord-172f9a9e1eff4016923928748d77ee2a
Quelldatensatz
uspto-grants-1992_02
Patentnummer
US05091553

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