Formaldehyde → n-Hexylhydroxymethylphosphinic acid, n-butyl ester

HRID 1539

Reaktionsgleichung

Reaktionsgleichung von HRID 1539
[CH2:1]([PH:7](=[O:13])[O:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].[CH2:14]=[O:15]>>[CH2:1]([P:7]([CH2:14][OH:15])(=[O:13])[O:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6]

Komponenten

3

Edukt 2

HCID 712FormaldehydeHCID 178418254HCID 178418254, Verbindung

Produkt 1

HCID 86752200n-Hexylhydroxymethylphosphinic acid, n-butyl ester

Versuchsvorschrift

The title compound was prepared from n-hexylphosphinic acid, n-butyl ester and paraformaldehyde according to the method described in Procedure 31. Purification by chromatography, eluting with dichloromethane containing 5% methanol, gave an oil.

Aufarbeitung

  1. customPurification by chromatography
  2. washeluting with dichloromethane containing 5% methanol
  3. customgave an oil

Quellen und Nachweise

ORD-Eintrag
ord-8ac817860d9d44d4acd7988671266af2
Quelldatensatz
uspto-grants-1998_03
Patentnummer
US05726165

Verknüpfte Notizen

Wird geladen…