HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl Thioglycolate → 6-Methoxy-benzo[B]thiophene-2-carboxylic acid methyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl Thioglycolate | HCID 16907 | — |
| Edukt | Sodium hydride | HCID 24758 | — |
| Edukt | 2-Fluoro-4-methoxybenzaldehyde | HCID 2734873 | — |
| Produkt | 6-Methoxy-benzo[B]thiophene-2-carboxylic acid methyl ester | HCID 53486111 | — |
Reaktionsschritte
Using 2.5 g (16.2 mmol) of 2-fluoro-4-methoxybenzaldehyde, 0.97 g (24.3 mmol) of sodium hydride (60% pure) and 1.89 g (17.8 mmol) of methyl mercaptoacetate, 3.05 g (84.7% of theory) of the title compound are obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07732477B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-743a5e0c9015488eb101d423a762ba83 |
| Quellennotiz | uspto-grants-2010_06 |