4-Chlorobenzenesulfonyl chloride → Benzyl(4-chlorobenzenesulfonyloxymethyl)phosphinic acid, n-butyl ester
Reaktionsgleichung
[CH2:1]([P:8]([CH2:15][OH:16])(=[O:14])[O:9][CH2:10][CH2:11][CH2:12][CH3:13])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[Cl:17][C:18]1[CH:23]=[CH:22][C:21]([S:24](Cl)(=[O:26])=[O:25])=[CH:20][CH:19]=1>>[CH2:1]([P:8]([CH2:15][O:16][S:24]([C:21]1[CH:22]=[CH:23][C:18]([Cl:17])=[CH:19][CH:20]=1)(=[O:26])=[O:25])(=[O:14])[O:9][CH2:10][CH2:11][CH2:12][CH3:13])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1Komponenten
3
Versuchsvorschrift
The title compound was prepared from benzylhydroxymethylphosphinic acid, n-butyl ester and 4-chlorobenzenesulfonyl chloride according to the method described in Procedure 32. The resulting white solid (mp 87°-88° C.) was used in the next stage without further purification.
Aufarbeitung
- customThe resulting white solid (mp 87°-88° C.) was used in the next stage without further purification