HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(4-tert-Butoxycarbonylamino-2-nitro-phenylamino)-acetic acid tert-butyl ester → HCID 67199974, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (4-tert-Butoxycarbonylamino-2-nitro-phenylamino)-acetic acid tert-butyl ester | HCID 67201113 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | HCID 67199974 | HCID 67199974 | — |
Reaktionsschritte
The product of step b.) (2.0 g, 5.45 mmol) was stirred with 3% Pd/C (200 mg) in ethanol (20 mL) under H2 (1 atm) for 90 minutes. The reaction was filtered over celite and concentrated to dryness to give the sub-title compound as a brown oil. This compound was used in crude form without purification. MS: ESI (positive): 338 (M+H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07732618B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-87a849f7a0c44fe2bcd1487199a27e08 |
| Quellennotiz | uspto-grants-2010_06 |