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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 15532Erstellt: 24. Oktober 2026

(4-tert-Butoxycarbonylamino-2-nitro-phenylamino)-acetic acid tert-butyl ester → HCID 67199974, Verbindung

https://huagongshe.com/de/reaction/15532

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt(4-tert-Butoxycarbonylamino-2-nitro-phenylamino)-acetic acid tert-butyl esterHCID 67201113—
KatalysatorPalladiumHCID 23938—
LösungsmittelEthanolHCID 702—
ProduktHCID 67199974HCID 67199974—

Reaktionsschritte

The product of step b.) (2.0 g, 5.45 mmol) was stirred with 3% Pd/C (200 mg) in ethanol (20 mL) under H2 (1 atm) for 90 minutes. The reaction was filtered over celite and concentrated to dryness to give the sub-title compound as a brown oil. This compound was used in crude form without purification. MS: ESI (positive): 338 (M+H).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07732618B2
Quelldatensatzuspto-grants-2010_06
ORD IDord-87a849f7a0c44fe2bcd1487199a27e08
Quellennotizuspto-grants-2010_06