Chlorotrimethylsilane → HCID 12472499, Verbindung

HRID 1576441Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1576441
[NH:1]1[CH2:5][CH2:4][NH:3][C:2]1=[S:6].[CH3:7][Si:8]([CH3:11])([CH3:10])Cl.C(N(CC)CC)C>O1CCCC1>[CH3:7][Si:8]([CH3:11])([CH3:10])[N:1]1[CH2:5][CH2:4][NH:3][C:2]1=[S:6]

Komponenten

5

Edukt 3

HCID 6397ChlorotrimethylsilaneHCID 8471TriethylamineHCID 2723650Ethylenethiourea

Produkt 1

HCID 12472499HCID 12472499, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 8028TetrahydrofuranLösungsmittel

Versuchsvorschrift

30.6 parts by weight of imidazolidine-2-thione were boiled overnight with 54.4 parts by weight of trimethylchlorosilane and 51.5 parts by weight of triethylamine in absolute tetrahydrofurane. The warm suspension was freed of the precipitated triethylamine hydrochloride by filtration, and the filtrate was evaporated and dried in a vacuum desiccator.

Aufarbeitung

  1. filtrationThe warm suspension was freed of the precipitated triethylamine hydrochloride by filtration
  2. customthe filtrate was evaporated
  3. customdried in a vacuum desiccator

Quellen und Nachweise

ORD-Eintrag
ord-607475582f614dde96533c3bbb62a64d
Quelldatensatz
uspto-grants-1976_09
Patentnummer
US03980792

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