5,6-Dimethoxy-1H-benzimidazol-2-amine → HCID 86734004, Verbindung
Reaktionsgleichung
[NH2:1][C:2]1[NH:3][C:4]2[CH:10]=[C:9]([O:11][CH3:12])[C:8]([O:13][CH3:14])=[CH:7][C:5]=2[N:6]=1.[Cl:15][CH2:16][S:17][C:18]1[CH:23]=[CH:22][CH:21]=[C:20]([I:24])[C:19]=1[Cl:25]>>[Cl-:15].[NH2:1][C:2]1[N:3]([CH2:16][S:17][C:18]2[CH:23]=[CH:22][CH:21]=[C:20]([I:24])[C:19]=2[Cl:25])[C:4]2[CH:10]=[C:9]([O:11][CH3:12])[C:8]([O:13][CH3:14])=[CH:7][C:5]=2[N+:6]=1[CH2:16][S:17][C:18]1[CH:23]=[CH:22][CH:21]=[C:20]([I:24])[C:19]=1[Cl:25]Komponenten
3
Versuchsvorschrift
Following the procedure of Example 2 and replacing 2-aminobenzimidazole with 2-amino-5,6-dimethoxybenzimidazole and replacing 2-bromo-4-chlorophenyl chloromethyl ether with 2-chloro-3-iodophenyl chloromethyl sulfide, the title compound is obtained.
Quellen und Nachweise
- ORD-Eintrag
- ord-5427029e5f344cf180ff0f384c56c37a
- Quelldatensatz
- uspto-grants-1976_09
- Patentnummer
- US03981886