4-(4-Methoxyphenyl)but-3-en-2-one → HCID 12374368, Verbindung

HRID 1577040

Reaktionsgleichung

Reaktionsgleichung von HRID 1577040
[Cl:1]([O-:5])(=[O:4])(=[O:3])=[O:2].[CH3:6][C:7]1[C:15]([CH3:17])([CH3:16])[C:14]2[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=2)[NH+:8]=1.[CH3:18][O:19][C:20]1[CH:25]=[CH:24][C:23]([CH:26]=[CH:27][C:28](=O)[CH3:29])=[CH:22][CH:21]=1>CO>[Cl:1]([O-:5])(=[O:4])(=[O:3])=[O:2].[CH3:29][C:28]1[N+:8]2[C:9]3[C:14]([C:15]([CH3:17])([CH3:16])[C:7]=2[CH:6]=[C:26]([C:23]2[CH:22]=[CH:21][C:20]([O:19][CH3:18])=[CH:25][CH:24]=2)[CH:27]=1)=[CH:13][CH:12]=[CH:11][CH:10]=3

Komponenten

4

Edukt 2

HCID 954144-(4-Methoxyphenyl)but-3-en-2-oneHCID 149131883H-Indole, 2,3,3-trimethyl-, perchlorate

Produkt 1

HCID 12374368HCID 12374368, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

2,3,3-Trimethyl-3H-indolium perchlorate (5 g.) and 4-p-methoxyphenylbut-3-ene-2-one (10 g.) were heated together on the steam bath for three hours. The cooled mixture was diluted with methanol and filtered. The product was purified by recrystallization from acetonitrile. Yield 4.1 g.; m.p. 298°-300° .

Aufarbeitung

  1. filtrationfiltered
  2. customThe product was purified by recrystallization from acetonitrile

Quellen und Nachweise

ORD-Eintrag
ord-10a387c8143d4b76b6e143ffaefdfae1
Quelldatensatz
uspto-grants-1976_09
Patentnummer
US03983288

Verknüpfte Notizen

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