HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Water → HCID 178457123, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Water | HCID 962 | — |
| Edukt | Allylamine | HCID 7853 | — |
| Edukt | Phosphorus pentachloride | HCID 24819 | — |
| Edukt | Methanone, (3-hydroxybenzo[b]thien-2-yl)phenyl- | HCID 4712192 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | HCID 178457123 | HCID 178457123 | 43% |
Reaktionsschritte
Prepared as in Example 1 from 2-benzoyl-benzo[b]thiophen-3-ol, phosphorus(V) chloride and a solution of one part by volume of allylamine in 2 parts by volume of water with a yield of 43% of theory. M.p. 104°-106° C. (ethyl acetate).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04288437 |
| Quelldatensatz | uspto-grants-1981_09 |
| ORD ID | ord-1b0dab7777a145188dd7f872712b4f3f |
| Quellennotiz | uspto-grants-1981_09 |