1,2,3,6-Tetrahydro-4-phenylpyridine → HCID 21559961, Verbindung
Reaktionsgleichung
[C:1]([N:4]1[C:12]2[C:7](=[CH:8][C:9]([O:13][CH3:14])=[CH:10][CH:11]=2)[CH:6]([CH2:15][CH2:16]Br)[CH:5]1[CH3:18])(=[O:3])[CH3:2].[C:19]1([C:25]2[CH2:26][CH2:27][NH:28][CH2:29][CH:30]=2)[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[C:1]([N:4]1[C:12]2[C:7](=[CH:8][C:9]([O:13][CH3:14])=[CH:10][CH:11]=2)[CH:6]([CH2:15][CH2:16][N:28]2[CH2:27][CH:26]=[C:25]([C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)[CH2:30][CH2:29]2)[CH:5]1[CH3:18])(=[O:3])[CH3:2]Komponenten
3
Versuchsvorschrift
In the manner described in Example 1, treatment of 1-acetyl-3-(2-bromoethyl)-5-methoxy-2-methylindoline with 1,2,3,6-tetrahydro-4-phenylpyridine gives white crystals, m.p. 113°-115°C., after recrystallization from dilute methanol.
Aufarbeitung
- customgives white crystals, m.p. 113°-115°C.
- customafter recrystallization from dilute methanol
Quellen und Nachweise
- ORD-Eintrag
- ord-e2a4894d948a44cfb7b027af9950e169