Methyl iodide → HCID 20560022, Verbindung

HRID 1579339Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1579339
[I-:1].[NH+]1C=CC=C[CH:3]=1.[CH:8]([NH:10][C:11]1[CH:24]=[CH:23][C:22]([O:25][CH3:26])=[CH:21][C:12]=1[CH2:13][CH2:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][N:16]=1)=[O:9].CI.C(NC1C=CC=CC=1CCC1C=CC=CN=1)=O>>[I-:1].[CH:8]([NH:10][C:11]1[CH:24]=[CH:23][C:22]([O:25][CH3:26])=[CH:21][C:12]=1[CH2:13][CH2:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][N+:16]=1[CH3:3])=[O:9]

Komponenten

5

Edukt 4

HCID 6328Methyl iodideHCID 20559958HCID 20559958, VerbindungHCID 20559985HCID 20559985, VerbindungHCID 21863515PyridiuM iodide

Produkt 1

HCID 20560022HCID 20560022, VerbindungAusbeute 95 %

Versuchsvorschrift

The pyridinium iodide is obtained by treating 2-(2-formamido-5-methoxyphenethyl)pyridine with methyl iodide according to the procedure described in Example 2c for 2-(o-formamidophenethyl)pyridine. Analytically pure 2-(2-formamido-5-methoxyphenethyl)-1-methylpyridinium iodide is obtained in a yield of 95% and has a melting point of 184°-186.5°C. (corr.).

Quellen und Nachweise

ORD-Eintrag
ord-d975ef4fd150411dabc346333fbe9872
Quelldatensatz
uspto-grants-1976_01
Patentnummer
US03931195

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