HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,3,4,5-Tetrahydropyridine → 2-Fluorenyl 2-pyrrolidinylmethyl ketone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,3,4,5-Tetrahydropyridine | HCID 68161 | — |
| Edukt | 2-Acetylfluorene | HCID 69908 | — |
| Edukt | 1-Pyrroline | HCID 79803 | — |
| Edukt | 2-Acetyldibenzofuran | HCID 293028 | — |
| Produkt | 2-Fluorenyl 2-pyrrolidinylmethyl ketone | HCID 12300793 | — |
Reaktionsschritte
Following essentially the same procedure as in Example XI above, but substituting 2-acetylfluorene for the 2-acetyldibenzofuran above and substituting 1-pyrroline as the trimer for the 2,3,4,5-tetrahydropyridine (as α-tripiperidein) above results in the formation of 2-fluorenyl 2-pyrrolidinylmethyl ketone as the hydrochloride salt, and which when recrystallized from isopropyl alcohol has a M.P. of 234-44°C. (dec.)
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US03931155 |
| Quelldatensatz | uspto-grants-1976_01 |
| ORD ID | ord-fb20cab4092b4b5e843807665404280b |
| Quellennotiz | uspto-grants-1976_01 |