Sulfuric Acid → 2-Amino-6-(3,4-dimethylphenyl)-6-methylheptane

HRID 1583835

Reaktionsgleichung

Reaktionsgleichung von HRID 1583835
[CH3:1][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][C:7]=1[CH3:8].S(=O)(=O)(O)O.[CH3:14][CH:15]([NH2:23])[CH2:16][CH2:17][CH2:18][C:19](O)([CH3:21])[CH3:20].Cl>CO>[NH2:23][CH:15]([CH2:16][CH2:17][CH2:18][C:19]([C:4]1[CH:5]=[CH:6][C:7]([CH3:8])=[C:2]([CH3:1])[CH:3]=1)([CH3:21])[CH3:20])[CH3:14]

Komponenten

5

Edukt 3

HCID 1118Sulfuric AcidHCID 7237O-XyleneHCID 10969Heptaminol Hydrochloride

Produkt 1

HCID 202585522-Amino-6-(3,4-dimethylphenyl)-6-methylheptane

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

21.2 Parts of o-xylene, 128 parts of 98% w/w sulphuric acid, 24 parts of methanol, and 36.3 parts of heptaminol hydrochloride were stirred at room temperature for 3 days. The work up was carried out as described in Example 2 and gave on distillation 36.2 parts of 2-amino-6-(3,4-dimethylphenyl)-6-methylheptane b16 164°-8° with the following percentage composition by weight.

Quellen und Nachweise

ORD-Eintrag
ord-2842386169e142f2a1a2f095751de616
Quelldatensatz
uspto-grants-1985_11
Patentnummer
US04554379

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