Diphenylmethane → Bis-(6-amino-2-methylhept-2-yl)diphenylmethane

HRID 1583837

Reaktionsgleichung

Reaktionsgleichung von HRID 1583837
[C:1]1([CH2:7][C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:14][CH:15]([NH2:23])[CH2:16][CH2:17][CH2:18][C:19](O)([CH3:21])[CH3:20].Cl>>[NH2:23][CH:15]([CH3:14])[CH2:16][CH2:17][CH2:18][C:19]([C:7]([C:19]([CH3:21])([CH2:18][CH2:17][CH2:16][CH:15]([NH2:23])[CH3:14])[CH3:20])([C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=1)[C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)([CH3:21])[CH3:20]

Komponenten

3

Edukt 2

HCID 7580DiphenylmethaneHCID 10969Heptaminol Hydrochloride

Produkt 1

HCID 20258548Bis-(6-amino-2-methylhept-2-yl)diphenylmethane

Versuchsvorschrift

16.8 parts of diphenylmethane were reacted with 36.4 parts of heptaminol hydrochloride according to the procedure of Example 2. Distillation gave 22.4 parts of bis-(6-amino-2-methylhept-2-yl)diphenylmethane b0.4 230°-44° C. Analysis of this fraction showed it to contain 73% of the 4,4'-isomer with the following percentage composition by weight

Aufarbeitung

  1. distillationDistillation

Quellen und Nachweise

ORD-Eintrag
ord-03e5d4ed2de44547b0309ab69d0badfc
Quelldatensatz
uspto-grants-1985_11
Patentnummer
US04554379

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