HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Methylimidazole → 1-((6-chloro-1,3-benzodioxol-5-yl)methyl)2-methyl-1H-imidazole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Methylimidazole | HCID 12749 | — |
| Edukt | Sodium hydride | HCID 24758 | — |
| Edukt | 6-Chloropiperonyl chloride | HCID 90113 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | 1-((6-chloro-1,3-benzodioxol-5-yl)methyl)2-methyl-1H-imidazole | HCID 21224807 | — |
Reaktionsschritte
The operation is carried out as in Stage 1 of Example 11 starting with 12.3 g of 2-methyl-1H-imidazole, 7.92 g of sodium hydride with 50% oil, 150 ml of N dimethylformamide and 33.8 g of 6-chloropiperonyl chloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05932741 |
| Quelldatensatz | uspto-grants-1999_08 |
| ORD ID | ord-6b398965cfb84cc889a194adca6f3e3c |
| Quellennotiz | uspto-grants-1999_08 |