HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1585286Erstellt: 26. Oktober 2026
Diethyl Ether → 2-[5-(2,6-Dimethoxyphenyl)-1-[4-[N-methyl-N-(3-dimethylaminopropyl)carbamoyl]-2-isopropylphenyl]-3-pyrazolylcarbonylamino]-2-adamantanecarboxylic acid benzenesulphonate
https://huagongshe.com/reaction/1585286
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Diethyl Ether | HCID 3283 | — |
| Edukt | Benzenesulfonic Acid | HCID 7371 | — |
| Edukt | SR142948A | HCID 5311451 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 2-[5-(2,6-Dimethoxyphenyl)-1-[4-[N-methyl-N-(3-dimethylaminopropyl)carbamoyl]-2-isopropylphenyl]-3-pyrazolylcarbonylamino]-2-adamantanecarboxylic acid benzenesulphonate | HCID 86754283 | 9,8% |
Reaktionsschritte
A mixture of 0.5 g of the compound obtained in EXAMPLE 1' and 0.16 g of benzenesulphonic acid in 5 ml of MeOH is poured into 75 ml of ether cooled to 5° C., and the precipitate formed is drained. 0.06 g of the expected product is obtained, m.p.=170° C. (dec.).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US05936123 |
|---|
| Quelldatensatz | uspto-grants-1999_08 |
|---|
| ORD ID | ord-076f15100bd444519e7dd5acc289824c |
|---|
| Quellennotiz | uspto-grants-1999_08 |
|---|
