Allyl Mercaptan → HCID 9794329, Verbindung

HRID 1585988Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1585988
[Na].[CH2:2]([SH:5])[CH:3]=[CH2:4].[CH3:6][O:7][C:8]1[N:9]=[N:10][C:11](Cl)=[C:12]([CH3:15])[C:13]=1[CH3:14]>CO>[CH3:6][O:7][C:8]1[N:9]=[N:10][C:11]([S:5][CH2:2][CH:3]=[CH2:4])=[C:12]([CH3:15])[C:13]=1[CH3:14]

Komponenten

5

Edukt 3

HCID 13367Allyl MercaptanHCID 5360545SodiumHCID 212176653-Chloro-6-methoxy-4,5-dimethylpyridazine

Produkt 1

HCID 9794329HCID 9794329, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

0.23 g(0.01 mol) of metallic sodium was dissolved in 30 ml of absolute methanol and then mixed with 0.93 ml(0.01 mol) of allylmercaptan. To this mixture was added 1.73 g(0.01 mol) of 3-methoxy-4,5-dimethyl-6-chloropyridazine obtained from Preparation 5. The reaction solution was refluxed for one hour and then treated according to the same manner as Example 1 to obtain the title compound as a freezing pale white crystal.

Aufarbeitung

  1. customobtained from Preparation 5
  2. temperatureThe reaction solution was refluxed for one hour
  3. additiontreated

Quellen und Nachweise

ORD-Eintrag
ord-ecd857d5b5914f38a47db573be880587
Quelldatensatz
uspto-grants-1999_08
Patentnummer
US05942511

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