Allyl Mercaptan → HCID 21217666, Verbindung

HRID 1585991Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1585991
[Na].[CH2:2]([SH:5])[CH:3]=[CH2:4].[CH2:6]([O:8][C:9]1[N:10]=[N:11][C:12](Cl)=[CH:13][CH:14]=1)[CH3:7]>CO>[CH2:6]([O:8][C:9]1[N:10]=[N:11][CH:12]=[CH:13][C:14]=1[S:5][CH2:2][CH:3]=[CH2:4])[CH3:7]

Komponenten

5

Edukt 3

HCID 13367Allyl MercaptanHCID 2615793-Chloro-6-ethoxypyridazineHCID 5360545Sodium

Produkt 1

HCID 21217666HCID 21217666, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

0.57 g(0.025 mol) of metallic sodium was dissolved in 40 ml of absolute methanol and then mixed with 2.49 ml(0.025 mol) of allylmercaptan. To this mixture was added 3.96 g(0.025 mol) of 3-ethoxy-6-chloropyridazine. The reaction solution was refluxed for 24 hours and then treated according to the same manner as Example 1 to obtain the title compound as a freezing pale white crystal.

Aufarbeitung

  1. temperatureThe reaction solution was refluxed for 24 hours
  2. additiontreated

Quellen und Nachweise

ORD-Eintrag
ord-b78a413db91a4584925d9e7c9d806fe9
Quelldatensatz
uspto-grants-1999_08
Patentnummer
US05942511

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