Allyl Mercaptan → HCID 9794857, Verbindung

HRID 1585994Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1585994
[Na].[CH2:2]([SH:5])[CH:3]=[CH2:4].[CH2:6]([O:8][C:9]1[C:18]2[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=2)[C:12](Cl)=[N:11][N:10]=1)[CH3:7]>CO>[CH2:6]([O:8][C:9]1[C:18]2[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=2)[C:12]([S:5][CH2:2][CH:3]=[CH2:4])=[N:11][N:10]=1)[CH3:7]

Komponenten

5

Edukt 3

HCID 13367Allyl MercaptanHCID 5360545SodiumHCID 212176601-Chloro-4-ethoxyphthalazine

Produkt 1

HCID 9794857HCID 9794857, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

0.23 g(0.01 mol) of metallic sodium was dissolved in 100 ml of absolute methanol and then mixed with 0.93 ml(0.01 mol) of allylmercaptan. To this mixture was added 2.09 g(0.01 mol) of 1-ethoxy-4-chlorophthalazine obtained from Preparation 10. The reaction solution was refluxed for 3 hours and then treated according to the same manner as Example 1 to obtain the title compound as a freezing white crystal.

Aufarbeitung

  1. customobtained from Preparation 10
  2. temperatureThe reaction solution was refluxed for 3 hours
  3. additiontreated

Quellen und Nachweise

ORD-Eintrag
ord-410766fcd3fc46009dbb63f29386785c
Quelldatensatz
uspto-grants-1999_08
Patentnummer
US05942511

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