Allyl Mercaptan → HCID 10130734, Verbindung

HRID 1585997Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1585997
[Na].[CH2:2]([SH:5])[CH:3]=[CH2:4].[CH2:6]([O:10][C:11]1[N:12]=[N:13][C:14](Cl)=[CH:15][CH:16]=1)[CH2:7][CH2:8][CH3:9]>CO>[CH2:6]([O:10][C:11]1[N:12]=[N:13][C:14]([S:5][CH2:2][CH:3]=[CH2:4])=[CH:15][CH:16]=1)[CH2:7][CH2:8][CH3:9]

Komponenten

5

Edukt 3

HCID 13367Allyl MercaptanHCID 2528253-butoxy-6-chloropyridazineHCID 5360545Sodium

Produkt 1

HCID 10130734HCID 10130734, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

1.15 g(0.05 mol) of metallic sodium was dissolved in 75 ml of absolute methanol and then mixed with 4.98 ml(0.05 mol) of allylmercaptan. To this mixture was added 9.33 g(0.05 mol) of 3-(n-butoxy)-6-chloropyridazine. The reaction solution was refluxed for 24 hours and then treated according to the same manner as Example 1 to obtain the title compound as a pale yellow oil.

Aufarbeitung

  1. temperatureThe reaction solution was refluxed for 24 hours
  2. additiontreated

Quellen und Nachweise

ORD-Eintrag
ord-c653d76dda1245b391a28e607699980c
Quelldatensatz
uspto-grants-1999_08
Patentnummer
US05942511

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