Allyl Mercaptan → HCID 21217662, Verbindung

HRID 1585999Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1585999
[Na].[CH2:2]([SH:5])[CH:3]=[CH2:4].[C:6]([O:10][C:11]1[N:12]=[N:13][C:14](Cl)=[CH:15][CH:16]=1)([CH3:9])([CH3:8])[CH3:7]>CO>[C:6]([O:10][C:11]1[N:12]=[N:13][C:14]([S:5][CH2:2][CH:3]=[CH2:4])=[CH:15][CH:16]=1)([CH3:9])([CH3:8])[CH3:7]

Komponenten

5

Edukt 3

HCID 13367Allyl MercaptanHCID 27639573-(Tert-Butoxy)-6-ChloropyridazineHCID 5360545Sodium

Produkt 1

HCID 21217662HCID 21217662, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

0.46 g(0.02 mol) of metallic sodium was dissolved in 30 ml of absolute methanol and then mixed with 1.99 ml(0.02 mol) of allylmercaptan. To this mixture was added 3.75 g(0.02 mol) of 3-(t-butoxy)-6-chloropyridazine. The reaction solution was refluxed for 24 hours and then treated according to the same manner as Example 1 to obtain the title compound as a pale yellow oil.

Aufarbeitung

  1. temperatureThe reaction solution was refluxed for 24 hours
  2. additiontreated

Quellen und Nachweise

ORD-Eintrag
ord-9c6696d76fa54e988979e37f461f3190
Quelldatensatz
uspto-grants-1999_08
Patentnummer
US05942511

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